Shales and applications in nuclear waste storage and petroleum industry


Gas Shales:

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Opportunities, Challenges and Achievements

Shales are fine-grained sedimentary geomaterials composed of clay minerals and tiny fragments (silt-sized particles) of other minerals, especially quartz and calcite. Shales are characterized by the presence of lamination and fissility which contribute in the development of a marked anisotropic behaviour. In addition, they are characterized by a very low permeability and good self-sealing potential; these properties make shales a suitable host material for many engineering applications. In this sense, the geomechanical behaviour of shales is quickly becoming one of the most important issues in modern geomechanics, largely driven by the nuclear waste geological storage and petroleum industries (i.e., the extraction of gas shale and the sequestration of CO2). In any such application, a deep understanding of the hydro-mechanical behaviour of the involved materials is of primary significance and it is indeed an exciting subject of research for the civil and environmental engineering society.
The water retention mechanisms play a major role in either fluid trapping due to the capillary forces present in low permeability reservoirs or in the resaturation of shale formations after ventilation, as in the case of deep geological repositories. The swelling/shrinkage of shale is related to suction, or the degree of saturation variations. New experimental methodologies have been recently developed at LMS for the analysis of the retention behaviour of shales (Laloui et al. 2012; Ferrari and Laloui, 2012); they involve the direct control of the shale water content and the subsequent measurement of the total suction by a psychrometer. Different techniques have also been considered at LMS for the volume measurement of the shale samples thus allowing the computation of the degree of saturation of the material.
The effects of a reduction of earth pressure on the surrounding material during the construction of a nuclear waste repository or the determination of the production capacity of shale gas reservoirs constitute some of the valuable geomechanical issues in this field of research; as a consequence, the mechanical properties and the permeability are challenging aspects to be investigated. Nonetheless, advanced testing devices have been recently developed at LMS thus providing the adequate equipment to face the mentioned challenges. In particular a high-pressure oedometer cell has been developed to analyse the hydro-mechanical behaviour of the geomaterials at high confining stresses (Salager et al. 2010; Ferrari and Laloui, 2012). The device can apply pressures up to 100 MPa; the high level of applicable vertical stress is required in order to observe the transition from the pre- to the post-yield behaviour of the material thus allowing for a mechanical characterization of the shales using methods similar to those applied to conventional soils. In order to analyse the settlement versus time curve, an analytical solution has been developed at LMS; it considers the time requested by the controller for applying the target pressure, the deformation of the apparatus, the primary consolidation settlement for a non-instantaneous loading and the secondary consolidation settlements.
A second aspect inspiring the research on shales for nuclear waste storage, shale gas and/or oil exploitation is the occurrence of high temperatures. At high depths and under high pressures, temperatures up to 100°C can be reached. The high-pressure oedometer cell presented above allows for the performance of tests in non-isothermal and controlled suction conditions. In addition, LMS is equipped with an innovative triaxial cell that can reproduce such temperatures, as well as extreme mechanical conditions, with an option for partial saturation (Seiphoori et al. 2010). LMS’s thermo-hydro-mechanical (THM) triaxial cell is especially designed for this kind of situations. Bore companies always search for efficient ways of exploitation. This affects also the engineers. One example of borehole improvement is the use of a drilling fluid, which is often water with dissolved salts. This fluid interacts with the soil with which it is in contact. In the case of partial saturation, the fluid can enter the pores of the material, for example. If saturated, a chemical gradient can result in osmotic pressures and flow of water, or diffusion of ions. All cases involve a change in the local chemistry of the pore fluid. LMS is currently researching the influence of salts on saturated soils and shales. Previous studies in the field of shale characterization focused mainly on (chemo-) poro-elasticity. LMS’s approach is developed in such a way that it provides the opportunity to consider irreversible strains as well (Witteveen et al. 2013). The mentioned points altogether form an advanced, unitary framework for the analysis of the thermo-hydro-chemo-mechanical behaviour of shales. LMS is convinced that its research adds valuable knowledge to the civil and environmental engineering community by profoundly researching the elasto-plasticity of this material.

Research group for shales:





PhD students

Research project

PhD Research Project

An effective stress framework for partially saturated gas shales: Kim Jinwoo

Gas shales are partially water saturated with their pore space simultaneously filled with brine and liquid and/or gas hydrocarbons. Changes in water saturation can cause swelling or shrinkage, which is of significant importance to natural gas production from unconventional shale reservoirs. During hydraulic fracturing, a substantial amount of injected water-based fluid is believed to imbibe into the shale matrix, driven by the high suction gradient between the well and the shale. However, currently available geomechanical models developed for reservoir problems are usually not multi-phase, and little is known about how suction and water saturation can be related to the resulting volumetric deformation in gas shales. This thesis will explore a possible effective stress framework for describing the swelling and shrinkage of gas shales as stress-strain behavior, including the non-linear hysteretic relationship between suction and water saturation. The outcome of this study is anticipated to provide insight into our understanding of the complex shale behavior and more efficient natural gas exploitation in the field.


E. Crisci, A. Ferrari, S. Giger, L. Laloui. Engineering Geology, 251, 214-227, 2019.

V. Favero, A. Ferrari and L. Laloui. Fourth EAGE Shale Workshop, Porto, Portugal, April 7-9, 2014.

V. Favero, F. Alessio and L. Lyesse. Géotechnique Symposium in Print 2013, London, UK.

A. Ferrari, V. Favero, D. Manca and L. Laloui. 47th US Rock Mechanics/Geomechanics Symposium, San Francisco (USA), 26-29 June 2013.

L. Laloui, A. Ferrari and S. Salager. 3rd EAGE Shale Workshop, Barcelona, 2012.

  •  New experimental tools for the characterization of highly overconsolidated clayey materials in unsaturated conditions, in Mechanics of unsaturated geomaterials,

S. Salager, A. Ferrari and L. Laloui. p. 113-126, 2010.

  •  An advanced calibration process for a thermo-hydro-mechanical triaxial system.

A. Seiphoori, A. Ferrari and L. Laloui. International Symposium on Deformation Characteristics of Geomaterials, Séoul, 2011.

  •  An experimental and constitutive investigation on the chemo-mechanical behaviour of a clay.

P. J. Witteveen, A. Ferrari and L. Laloui. Geotechnique -London-, vol. 63, num. 3, p. 244–255, 2013.

  • Advances in the Testing of the Hydro-mechanical Behaviour of Shales.

A. Ferrari and L. Laloui. Springer Series in Geomechanics and Geoengineering, 2012.